Bio-nanocomposite films reinforced with cellulose nanocrystals: Rheology of film-forming solutions, transparency, water vapor barrier and tensile properties of films.
Identifieur interne : 001877 ( Main/Exploration ); précédent : 001876; suivant : 001878Bio-nanocomposite films reinforced with cellulose nanocrystals: Rheology of film-forming solutions, transparency, water vapor barrier and tensile properties of films.
Auteurs : Nassima El Miri [Maroc] ; Karima Abdelouahdi [Maroc] ; Abdellatif Barakat [France] ; Mohamed Zahouily [Maroc] ; Aziz Fihri [Maroc] ; Abderrahim Solhy [Maroc] ; Mounir El Achaby [Maroc]Source :
- Carbohydrate polymers [ 1879-1344 ] ; 2015.
Descripteurs français
- KwdFr :
- MESH :
English descriptors
- KwdEn :
- Alkalies (chemistry), Cellulose (chemistry), Elasticity, Nanocomposites (chemistry), Nanoparticles (chemistry), Permeability, Rheology, Saccharum (chemistry), Solutions, Spectrophotometry, Ultraviolet, Spectroscopy, Fourier Transform Infrared, Starch (chemistry), Steam (analysis), Tensile Strength, Viscosity.
- MESH :
- chemical , analysis : Steam.
- chemical , chemistry : Alkalies, Cellulose, Starch.
- chemistry : Nanocomposites, Nanoparticles, Saccharum.
- Elasticity, Permeability, Rheology, Solutions, Spectrophotometry, Ultraviolet, Spectroscopy, Fourier Transform Infrared, Tensile Strength, Viscosity.
Abstract
This study was aimed to develop bio-nanocomposite films of carboxymethyl cellulose (CMC)/starch (ST) polysaccharide matrix reinforced with cellulose nanocrystals (CNC) using the solution casting method. The CNC were extracted at the nanometric scale from sugarcane bagasse via sulfuric acid hydrolysis and used as reinforcing phase to produce CMC/ST-CNC bio-nanocomposite films at different CNC loading levels (0.5-5.0 wt%). Steady shear viscosity and dynamic viscoelastic measurements of film-forming solution (FFS) of neat CMC, CMC/ST blend and CMC/ST-CNC bio-nanocomposites were evaluated. Viscosity measurements revealed that a transition from Newtonian behavior to shear thinning occurred when CNC were added. The dynamic tests confirmed that all FFS have a viscoelastic behavior with an entanglement network structure, induced by the hydrogen bonding. In regard to the cast film quality, the rheological data showed that all FFS were suitable for casting of films at ambient temperature. The effect of CNC addition on the optical transparency, water vapor permeability (WVP) and tensile properties of bio-nanocomposite films was studied. It was found that bio-nanocomposite films remain transparent due to CNC dispersion at the nanoscale. The WVP was significantly reduced and the elastic modulus and tensile strength were increased gradually with the addition of CNC. Herein, the steps to form new eco-friendly bio-nanocomposite films were described by taking advantage of the combination of CMC, ST and CNC. The as-produced films exhibited good optical transparency, reduced WVP and enhanced tensile properties, which are the main properties required for packaging applications.
DOI: 10.1016/j.carbpol.2015.04.051
PubMed: 26050901
Affiliations:
- France, Maroc
- Languedoc-Roussillon, Occitanie (région administrative), Rabat-Salé-Kénitra
- Montpellier, Rabat
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Le document en format XML
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MAScIR Foundation, Rabat Design, Rue Mohamed El Jazouli, Madinat Al Irfane, 10100 Rabat, Morocco.</nlm:affiliation><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratoire de Matériaux, Catalyse & Valorisation des Ressources Naturelles, FST Mohammedia, Université Hassan II de Casablanca, Rue Tarik Bnou Ziad, Mers Sultan, 9167 Casablanca, Morocco; MAScIR Foundation, Rabat Design, Rue Mohamed El Jazouli, Madinat Al Irfane, 10100 Rabat</wicri:regionArea><placeName><settlement type="city">Rabat</settlement><region nuts="2">Rabat-Salé-Kénitra</region></placeName></affiliation></author><author><name sortKey="Abdelouahdi, Karima" sort="Abdelouahdi, Karima" uniqKey="Abdelouahdi K" first="Karima" last="Abdelouahdi">Karima Abdelouahdi</name><affiliation wicri:level="1"><nlm:affiliation>Division UATRS, Centre National pour la Recherche Scientifique et Technique (CNRST), Angle Allal Fassi/FAR, Hay Riad, 10100 Rabat, Morocco.</nlm:affiliation><country xml:lang="fr">Maroc</country><wicri:regionArea>Division UATRS, Centre National pour la Recherche Scientifique et Technique (CNRST), Angle Allal Fassi/FAR, Hay Riad, 10100 Rabat</wicri:regionArea><placeName><settlement type="city">Rabat</settlement><region nuts="2">Rabat-Salé-Kénitra</region></placeName></affiliation></author><author><name sortKey="Barakat, Abdellatif" sort="Barakat, Abdellatif" uniqKey="Barakat A" first="Abdellatif" last="Barakat">Abdellatif Barakat</name><affiliation wicri:level="3"><nlm:affiliation>INRA, UMR 1208 Ingénierie des Agropolymères et Technologies Emergentes (IATE), 2, place Pierre Viala, 34060 Montpellier Cedex 1, France.</nlm:affiliation><country xml:lang="fr">France</country><wicri:regionArea>INRA, UMR 1208 Ingénierie des Agropolymères et Technologies Emergentes (IATE), 2, place Pierre Viala, 34060 Montpellier Cedex 1</wicri:regionArea><placeName><region type="region" nuts="2">Occitanie (région administrative)</region><region type="old region" nuts="2">Languedoc-Roussillon</region><settlement type="city">Montpellier</settlement></placeName></affiliation></author><author><name sortKey="Zahouily, Mohamed" sort="Zahouily, Mohamed" uniqKey="Zahouily M" first="Mohamed" last="Zahouily">Mohamed Zahouily</name><affiliation wicri:level="1"><nlm:affiliation>Laboratoire de Matériaux, Catalyse & Valorisation des Ressources Naturelles, FST Mohammedia, Université Hassan II de Casablanca, Rue Tarik Bnou Ziad, Mers Sultan, 9167 Casablanca, Morocco; MAScIR Foundation, Rabat Design, Rue Mohamed El Jazouli, Madinat Al Irfane, 10100 Rabat, Morocco.</nlm:affiliation><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratoire de Matériaux, Catalyse & Valorisation des Ressources Naturelles, FST Mohammedia, Université Hassan II de Casablanca, Rue Tarik Bnou Ziad, Mers Sultan, 9167 Casablanca, Morocco; MAScIR Foundation, Rabat Design, Rue Mohamed El Jazouli, Madinat Al Irfane, 10100 Rabat</wicri:regionArea><placeName><settlement type="city">Rabat</settlement><region nuts="2">Rabat-Salé-Kénitra</region></placeName></affiliation></author><author><name sortKey="Fihri, Aziz" sort="Fihri, Aziz" uniqKey="Fihri A" first="Aziz" last="Fihri">Aziz Fihri</name><affiliation wicri:level="1"><nlm:affiliation>MAScIR Foundation, Rabat Design, Rue Mohamed El Jazouli, Madinat Al Irfane, 10100 Rabat, Morocco.</nlm:affiliation><country xml:lang="fr">Maroc</country><wicri:regionArea>MAScIR Foundation, Rabat Design, Rue Mohamed El Jazouli, Madinat Al Irfane, 10100 Rabat</wicri:regionArea><placeName><settlement type="city">Rabat</settlement><region nuts="2">Rabat-Salé-Kénitra</region></placeName></affiliation></author><author><name sortKey="Solhy, Abderrahim" sort="Solhy, Abderrahim" uniqKey="Solhy A" first="Abderrahim" last="Solhy">Abderrahim Solhy</name><affiliation wicri:level="1"><nlm:affiliation>Center For Advanced Materials, Université Mohammed VI Polytechnique, Lot 660-Hay Moulay Rachid, 43150 Ben Guerir, Morocco. Electronic address: abderrahim.solhy@um6p.ma.</nlm:affiliation><country xml:lang="fr">Maroc</country><wicri:regionArea>Center For Advanced Materials, Université Mohammed VI Polytechnique, Lot 660-Hay Moulay Rachid, 43150 Ben Guerir</wicri:regionArea><wicri:noRegion>43150 Ben Guerir</wicri:noRegion></affiliation></author><author><name sortKey="El Achaby, Mounir" sort="El Achaby, Mounir" uniqKey="El Achaby M" first="Mounir" last="El Achaby">Mounir El Achaby</name><affiliation wicri:level="1"><nlm:affiliation>Center For Advanced Materials, Université Mohammed VI Polytechnique, Lot 660-Hay Moulay Rachid, 43150 Ben Guerir, Morocco. Electronic address: Mounir.elachaby@um6p.ma.</nlm:affiliation><country xml:lang="fr">Maroc</country><wicri:regionArea>Center For Advanced Materials, Université Mohammed VI Polytechnique, Lot 660-Hay Moulay Rachid, 43150 Ben Guerir</wicri:regionArea><wicri:noRegion>43150 Ben Guerir</wicri:noRegion></affiliation></author></analytic><series><title level="j">Carbohydrate polymers</title><idno type="eISSN">1879-1344</idno><imprint><date when="2015" type="published">2015</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Alkalies (chemistry)</term><term>Cellulose (chemistry)</term><term>Elasticity</term><term>Nanocomposites (chemistry)</term><term>Nanoparticles (chemistry)</term><term>Permeability</term><term>Rheology</term><term>Saccharum (chemistry)</term><term>Solutions</term><term>Spectrophotometry, Ultraviolet</term><term>Spectroscopy, Fourier Transform Infrared</term><term>Starch (chemistry)</term><term>Steam (analysis)</term><term>Tensile Strength</term><term>Viscosity</term></keywords><keywords scheme="KwdFr" xml:lang="fr"><term>Alcalis ()</term><term>Amidon ()</term><term>Cellulose ()</term><term>Nanocomposites ()</term><term>Nanoparticules ()</term><term>Perméabilité</term><term>Rhéologie</term><term>Résistance à la traction</term><term>Saccharum ()</term><term>Solutions</term><term>Spectrophotométrie UV</term><term>Spectroscopie infrarouge à transformée de Fourier</term><term>Vapeur (analyse)</term><term>Viscosité</term><term>Élasticité</term></keywords><keywords scheme="MESH" type="chemical" qualifier="analysis" xml:lang="en"><term>Steam</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Alkalies</term><term>Cellulose</term><term>Starch</term></keywords><keywords scheme="MESH" qualifier="analyse" xml:lang="fr"><term>Vapeur</term></keywords><keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Nanocomposites</term><term>Nanoparticles</term><term>Saccharum</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Elasticity</term><term>Permeability</term><term>Rheology</term><term>Solutions</term><term>Spectrophotometry, Ultraviolet</term><term>Spectroscopy, Fourier Transform Infrared</term><term>Tensile Strength</term><term>Viscosity</term></keywords><keywords scheme="MESH" xml:lang="fr"><term>Alcalis</term><term>Amidon</term><term>Cellulose</term><term>Nanocomposites</term><term>Nanoparticules</term><term>Perméabilité</term><term>Rhéologie</term><term>Résistance à la traction</term><term>Saccharum</term><term>Solutions</term><term>Spectrophotométrie UV</term><term>Spectroscopie infrarouge à transformée de Fourier</term><term>Viscosité</term><term>Élasticité</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">This study was aimed to develop bio-nanocomposite films of carboxymethyl cellulose (CMC)/starch (ST) polysaccharide matrix reinforced with cellulose nanocrystals (CNC) using the solution casting method. The CNC were extracted at the nanometric scale from sugarcane bagasse via sulfuric acid hydrolysis and used as reinforcing phase to produce CMC/ST-CNC bio-nanocomposite films at different CNC loading levels (0.5-5.0 wt%). Steady shear viscosity and dynamic viscoelastic measurements of film-forming solution (FFS) of neat CMC, CMC/ST blend and CMC/ST-CNC bio-nanocomposites were evaluated. Viscosity measurements revealed that a transition from Newtonian behavior to shear thinning occurred when CNC were added. The dynamic tests confirmed that all FFS have a viscoelastic behavior with an entanglement network structure, induced by the hydrogen bonding. In regard to the cast film quality, the rheological data showed that all FFS were suitable for casting of films at ambient temperature. The effect of CNC addition on the optical transparency, water vapor permeability (WVP) and tensile properties of bio-nanocomposite films was studied. It was found that bio-nanocomposite films remain transparent due to CNC dispersion at the nanoscale. The WVP was significantly reduced and the elastic modulus and tensile strength were increased gradually with the addition of CNC. Herein, the steps to form new eco-friendly bio-nanocomposite films were described by taking advantage of the combination of CMC, ST and CNC. The as-produced films exhibited good optical transparency, reduced WVP and enhanced tensile properties, which are the main properties required for packaging applications.</div></front></TEI><affiliations><list><country><li>France</li><li>Maroc</li></country><region><li>Languedoc-Roussillon</li><li>Occitanie (région administrative)</li><li>Rabat-Salé-Kénitra</li></region><settlement><li>Montpellier</li><li>Rabat</li></settlement></list><tree><country name="Maroc"><region name="Rabat-Salé-Kénitra"><name sortKey="El Miri, Nassima" sort="El Miri, Nassima" uniqKey="El Miri N" first="Nassima" last="El Miri">Nassima El Miri</name></region><name sortKey="Abdelouahdi, Karima" sort="Abdelouahdi, Karima" uniqKey="Abdelouahdi K" first="Karima" last="Abdelouahdi">Karima Abdelouahdi</name><name sortKey="El Achaby, Mounir" sort="El Achaby, Mounir" uniqKey="El Achaby M" first="Mounir" last="El Achaby">Mounir El Achaby</name><name sortKey="Fihri, Aziz" sort="Fihri, Aziz" uniqKey="Fihri A" first="Aziz" last="Fihri">Aziz Fihri</name><name sortKey="Solhy, Abderrahim" sort="Solhy, Abderrahim" uniqKey="Solhy A" first="Abderrahim" last="Solhy">Abderrahim Solhy</name><name sortKey="Zahouily, Mohamed" sort="Zahouily, Mohamed" uniqKey="Zahouily M" first="Mohamed" last="Zahouily">Mohamed Zahouily</name></country><country name="France"><region name="Occitanie (région administrative)"><name sortKey="Barakat, Abdellatif" sort="Barakat, Abdellatif" uniqKey="Barakat A" first="Abdellatif" last="Barakat">Abdellatif Barakat</name></region></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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